Hydrothermal and Electrochemical Synthesis of <i>MoS₂</i> Nanoparticles and Their Characterization

Abstract

UDC 538.9

DOI  https://doi.org/10.5281/zenodo.2551248

The features of the hydrothermal synthesis (molybdenum precursor – Na₂MoO₄, sulfur precursor – thioacetamide, temperature – 220°C) and of the electrochemical one (anodic formation of nanoparticles from MoS₂ single crystals at electrolysis in ionic liquid) are described. The X-ray fluorescence, optical absorption, and photoluminescence spectroscopy were applied for their characterization.

Keywords: molybdenum sulfide, nanoparticles, hydrothermal synthesis, electrolisis in ionic liquids, photoluminescence spectroscopy.